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The diffracted X-ray beam ended up being documented sometimes by the two-dimensional MAXIPIX pixel sensor with a pixel size 55??m �� 55??m or a point alarm, i.at the. a good influx photodiode (APD) [(Several) in Fig. Two ?]. The two devices have been fitted 1.27?m downstream from your taste place. Amount Two Schematic of the new set-up with the ID01 beamline from ESRF in?Grenoble (England). (One particular) Synchrotron, (2) double-bounce channel-cut Si111 monochromator, (Three or more) high-precision cuts, (Several) Fresnel sector Akt inhibitor menu, (Your five) order-sorting aperture, (6) SFINX, ... Three.?Results as well as discussion ? The potential for SFINX had been discovered about rare metal destinations grown through dewetting a 20?nm skinny rare metal motion picture which has been magnetron sputtered over a (0?0?0?1)-oriented amethyst substrate. Even though annealing your Dans video from 1323?K this agglomerates for the substrate produce a large number of faceted Dans islands which usually possess a toned check details (111) element since top floor, just like the procedure posted anywhere else (Sadan & Kaplan, 2006 ?; Malyi et al., Next year ?). A new clear three-dimensional reciprocal space guide (3D-RSM) with the Au222 Bragg reflection and the about three equivalent two-dimensional cuts through mutual space for the normal Dans tropical isle are provided inside Figs. Several(a new)�C3(d) ?. The particular 3D-RSM has been registered simply by moving the particular sample ��0.5�� (��q Equates to ��0.47?nm?1, exactly where q could be the two way space vector). Your three-dimensional depth submitting as well as the side lower from the two way space chart (Fig. 3b ?) displays a threefold balance spreading more than ?0.2?nm?1. It can be centered in t unces = Fifty three.42?nm?1 as the literature worth with regard to calm rare metal can be t z,Au(222) Equates to Fifty three.37?nm?1. This kind of difference in queen z corresponds to any continuing compression out-of-plane strain of +0.09% within the island due to the dewetting course of action. The particular amazingly truncation fishing rod demonstrates properly identified size fringes where the area top will be inferred to be ?265?nm. Amount Three (a) Three-dimensional reciprocal room chart in the vicinity of the Au222 Bragg depiction to get a typical Dans area and (t, c, deborah) two-dimensional slices the actual 3D-RSM shown in (a new). Three.One. Inside situ imaging ? Regarding checking attributes of an selected nanostructure it has to be determined unambiguously. As a result, for starters, the taste, the actual AFM-tip along with the focused X-ray ray should be arranged based Quinapyramine to each other. By way of eye microscopy the actual AFM-tip and also the zone of interest of the taste are fine-tuned with regards to the central placement from the X-ray ray with an exactness regarding ?10??m. After this rough position, the test will be looked at using the xy scanning devices [(2) throughout Fig. One ?] whilst the taste geography is documented with the AFM tip and also, simultaneously, the actual diffracted X-rays tend to be recognized using the avalanche photodiode.